摘要: 基于X射线衍射(XRD)法、偏光显微镜(PLM) 法和扫描电镜能谱(SEM/EDS) 法3种技术对涂料及其相关材料中石棉的检测展开系统的研究,由于每种方法都有其优越性和局限性,因此几种方法相互辅证,取长补短,才能使结果更加准确。 文中根据每种方法的特点,从样品前处理、样品制备和分析过程等方面分别进行讨论,并对结果的分析方法做出详细的说明。
关键词:
涂料,
石棉,
X 射线衍射,
偏光显微镜,
扫描电镜能谱
Abstract: A systematic research on methods based on X-ray diffraction (XRD) polarizing microscope (PLM) and scanning electron microscopy/energy dispersive spectrometer(SEM/EDS) for determination of asbestos in coatings has been carried out. Because different method has its different advantages and disadvantages, a synergy of the several methods should be taken so as to Improve the accuracy of the testing result. According to the characteristics of every method, a detailed discussion is provided in terms of sample pretreatment and preparation as well as analyzing process, etc. Meanwhile, the analyzing method of the result is described in detail.
Key words:
coatings,
asbestos,
x-ray diffraction polarizing microscope,
scanning electron microscope/energy dispersive spectrometer
王玉鹏, 季军宏, 唐佳瑜, 万雪期, 彭菊芳. 涂料及其相关材料中石棉测定方法的研究[J]. 涂料工业, 2016, 46(2): 53-58.
Wang Yupeng, Ji Junhong, Tang Jiayu, Wan Xueqi, Peng Jufang. Research on Methods for Determination of Asbestos
in Coatings and Related Materials[J]. Paint & Coatings Industry, 2016, 46(2): 53-58.