涂料工业 ›› 2016, Vol. 46 ›› Issue (2): 53-58.

• 标准及检测 • 上一篇    下一篇

涂料及其相关材料中石棉测定方法的研究

王玉鹏,季军宏,唐佳瑜,万雪期,彭菊芳   

  1. 中海油常州涂料化工研究院有限公司,江苏常州 213016
  • 出版日期:2016-02-29 发布日期:2019-06-01
  • 基金资助:
    消费品中化学危害共性安全标准及 10 类重点产品关键技术标准研制(涂料)(项目号:201510203-05)

Research on Methods for Determination of Asbestos in Coatings and Related Materials

Wang Yupeng, Ji Junhong, Tang Jiayu, Wan Xueqi, Peng Jufang   

  1. CNOOC Changzhou Paint Coatings Industry Research Institute,Co., Ltd., Changzhou, Jiangsu 213016, China
  • Online:2016-02-29 Published:2019-06-01

摘要: 基于X射线衍射(XRD)法、偏光显微镜(PLM) 法和扫描电镜能谱(SEM/EDS) 法3种技术对涂料及其相关材料中石棉的检测展开系统的研究,由于每种方法都有其优越性和局限性,因此几种方法相互辅证,取长补短,才能使结果更加准确。 文中根据每种方法的特点,从样品前处理、样品制备和分析过程等方面分别进行讨论,并对结果的分析方法做出详细的说明。

关键词: 涂料, 石棉, X 射线衍射, 偏光显微镜, 扫描电镜能谱

Abstract: A systematic research on methods based on X-ray diffraction (XRD) polarizing microscope (PLM) and scanning electron microscopy/energy dispersive spectrometer(SEM/EDS) for determination of asbestos in coatings has been carried out. Because different method has its different advantages and disadvantages, a synergy of the several methods should be taken so as to Improve the accuracy of the testing result. According to the characteristics of every method, a detailed discussion is provided in terms of sample pretreatment and preparation as well as analyzing process, etc. Meanwhile, the analyzing method of the result is described in detail.

Key words: coatings, asbestos, x-ray diffraction polarizing microscope, scanning electron microscope/energy dispersive spectrometer